Crystal data collection and refinement statistics
| . | STK19 SeMet dataset . |
|---|---|
| Cell axial lengths (Å) | a = 55.3, b = 96.6, c = 98.8, α = β = γ = 90 |
| Spacegroup | P212121 |
| Data collection | |
| Resolution range (Å) | 50.00–1.65 (1.69–1.65) |
| Number of observed reflections | 800,904 (45,192) |
| Number of unique reflections | 64,082 (4,673) |
| Completeness (%) | 99.3 (99.2) |
| Multiplicity | 12.5 (9.7) |
| Anomalous completeness | 99.1 (98.9) |
| Anomalous multiplicity | 6.5 (5.0) |
| Rpim | 0.019 (0.310) |
| CC1/2 | 0.999 (0.821) |
| Mean I/Isigma | 26.1 (2.4) |
| Refinement | |
| Resolution range (Å) | 50.0–1.65 (1.69–1.65) |
| Number of working reflections | 60,759 (4,453) |
| Number of test reflections | 3,247 (216) |
| Rwork | 0.149 (0.233) |
| Rfree | 0.194 (0.333) |
| R.m.s. deviation bond lengths (Å) | 0.007 |
| R.m.s. deviation bond angles (°) | 1.487 |
| Average B-factors (Å2) (# of atoms) | 36.5 (3,918) |
| Ramachandran plot | |
| Favored regions (%) | 97.0 |
| General allowed regions (%) | 3.0 |
| Disallowed regions (%) | 0.0 |
| . | STK19 SeMet dataset . |
|---|---|
| Cell axial lengths (Å) | a = 55.3, b = 96.6, c = 98.8, α = β = γ = 90 |
| Spacegroup | P212121 |
| Data collection | |
| Resolution range (Å) | 50.00–1.65 (1.69–1.65) |
| Number of observed reflections | 800,904 (45,192) |
| Number of unique reflections | 64,082 (4,673) |
| Completeness (%) | 99.3 (99.2) |
| Multiplicity | 12.5 (9.7) |
| Anomalous completeness | 99.1 (98.9) |
| Anomalous multiplicity | 6.5 (5.0) |
| Rpim | 0.019 (0.310) |
| CC1/2 | 0.999 (0.821) |
| Mean I/Isigma | 26.1 (2.4) |
| Refinement | |
| Resolution range (Å) | 50.0–1.65 (1.69–1.65) |
| Number of working reflections | 60,759 (4,453) |
| Number of test reflections | 3,247 (216) |
| Rwork | 0.149 (0.233) |
| Rfree | 0.194 (0.333) |
| R.m.s. deviation bond lengths (Å) | 0.007 |
| R.m.s. deviation bond angles (°) | 1.487 |
| Average B-factors (Å2) (# of atoms) | 36.5 (3,918) |
| Ramachandran plot | |
| Favored regions (%) | 97.0 |
| General allowed regions (%) | 3.0 |
| Disallowed regions (%) | 0.0 |