Table 1.

Data collection and refinement statistics

Data CrIFT70FL/52330–381 CrIFT70FL/52330–381 TtIFT52540–603/46236–347 TtIFT52540–603/46236–347 
 Native data KAu(CN)2 soak Native data KAu(CN)2 soak 
Data collection     
Space group P63 P63 P3221 P3221 
Unit cell/Å a = b = 143.2, c = 88.7 a = b = 143.2, c = 88.7 a = b = 84.3, c = 95.5 a = b = 84.9, c = 95.2 
Resolution/Å 50–2.5 (2.65–2.50) 50–2.5 (2.65–2.50) 40–2.3 (2.4–2.3) 50–2.8 (2.9–2.8) 
I/sigma (I) 17.7 (1.3) 8.0 (1.1) 17.0 (0.6) 20.2 (2.0) 
R-meas 0.095 (1.83) 0.152 (1.16) 0.072 (3.21) 0.09 (0.95) 
CC (1/2) 0.999 (0.481) 0.995 (0.385) 1.0 (0.54) 1.0 (0.90) 
Completeness 0.995 (0.972) 0.993 (0.981) 0.988 (0.929) 0.982 (0.891) 
Anomalous signal None 4.5 Å None 3.7 Å 
Data refinement     
Resolution/Å 50–2.5 (2.53–2.50)  40–2.32 (2.46–2.3)  
No of reflections (free test set) 35,954 (1758)  17,160 (878)  
Rwork 0.172 (0.273)  0.218 (0.391)  
Rfree 0.236 (0.317)  0.252 (0.453)  
RMSD bonds 0.008Å  0.009Å  
RMSD angles 1.1°  1.24°  
Ramachandran plot     
Favored 94.0%  95.3%  
Allowed 5.4%  2.9%  
Outliers 0.6%  0.6%  
Data CrIFT70FL/52330–381 CrIFT70FL/52330–381 TtIFT52540–603/46236–347 TtIFT52540–603/46236–347 
 Native data KAu(CN)2 soak Native data KAu(CN)2 soak 
Data collection     
Space group P63 P63 P3221 P3221 
Unit cell/Å a = b = 143.2, c = 88.7 a = b = 143.2, c = 88.7 a = b = 84.3, c = 95.5 a = b = 84.9, c = 95.2 
Resolution/Å 50–2.5 (2.65–2.50) 50–2.5 (2.65–2.50) 40–2.3 (2.4–2.3) 50–2.8 (2.9–2.8) 
I/sigma (I) 17.7 (1.3) 8.0 (1.1) 17.0 (0.6) 20.2 (2.0) 
R-meas 0.095 (1.83) 0.152 (1.16) 0.072 (3.21) 0.09 (0.95) 
CC (1/2) 0.999 (0.481) 0.995 (0.385) 1.0 (0.54) 1.0 (0.90) 
Completeness 0.995 (0.972) 0.993 (0.981) 0.988 (0.929) 0.982 (0.891) 
Anomalous signal None 4.5 Å None 3.7 Å 
Data refinement     
Resolution/Å 50–2.5 (2.53–2.50)  40–2.32 (2.46–2.3)  
No of reflections (free test set) 35,954 (1758)  17,160 (878)  
Rwork 0.172 (0.273)  0.218 (0.391)  
Rfree 0.236 (0.317)  0.252 (0.453)  
RMSD bonds 0.008Å  0.009Å  
RMSD angles 1.1°  1.24°  
Ramachandran plot     
Favored 94.0%  95.3%  
Allowed 5.4%  2.9%  
Outliers 0.6%  0.6%  

Numbers in parentheses are for the highest resolution shell.

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