Table 2.

Vt–PIP2 crystallographic refinement statistics

Statistics Overall Last shell 
Resolution 45.17–3.20 Å 3.37–3.2 Å 
No. reflections (working set) 18,212 2,594 
No. of reflections (test set) 967 144 
Rwork/Rfree 0.206/0.253 0.235/0.277 
No. atoms   
Protein 8,090  
PIP2 141  
Solvent 75  
B-factors   
Protein 147 Å2  
PIP2 235 Å2  
Solvent 92 Å2  
Root mean square deviations   
Bond lengths 0.010 Å  
Bond angles 1.11°  
Ramachandran plot   
Favored 96.95%  
Allowed 3.05%  
Generously allowed 0%  
Outliers 0%  
Statistics Overall Last shell 
Resolution 45.17–3.20 Å 3.37–3.2 Å 
No. reflections (working set) 18,212 2,594 
No. of reflections (test set) 967 144 
Rwork/Rfree 0.206/0.253 0.235/0.277 
No. atoms   
Protein 8,090  
PIP2 141  
Solvent 75  
B-factors   
Protein 147 Å2  
PIP2 235 Å2  
Solvent 92 Å2  
Root mean square deviations   
Bond lengths 0.010 Å  
Bond angles 1.11°  
Ramachandran plot   
Favored 96.95%  
Allowed 3.05%  
Generously allowed 0%  
Outliers 0%  

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