Table 1.

X-ray data collection and refinement statistics

Variable Value 
Data collection  
Space group P21 
Cell dimensions  
a, b, c 46.86, 82.39, and 83.40Å 
 α, β, γ 90, 95.2, and 90° 
Wavelength 0.9790 
Resolution 50.0–2.35Å 
Rsym or Rmerge 5.9 (27.5)a 
II 19 (3.2)a 
Completeness 91.7% (98.3%)a 
Redundancy 2.9 
Refinement  
Resolution 2.35Å 
No. reflections 22,885 
Rwork/Rfree 23.0/27.5 
Number of atoms  
 Protein 4,004 
 Solvent 260 
B factors  
 Protein 17.5 
 Solvent 21.2 
R.m.s deviations  
 Bond lengths 0.006Å 
 Bond angles 0.88° 
Variable Value 
Data collection  
Space group P21 
Cell dimensions  
a, b, c 46.86, 82.39, and 83.40Å 
 α, β, γ 90, 95.2, and 90° 
Wavelength 0.9790 
Resolution 50.0–2.35Å 
Rsym or Rmerge 5.9 (27.5)a 
II 19 (3.2)a 
Completeness 91.7% (98.3%)a 
Redundancy 2.9 
Refinement  
Resolution 2.35Å 
No. reflections 22,885 
Rwork/Rfree 23.0/27.5 
Number of atoms  
 Protein 4,004 
 Solvent 260 
B factors  
 Protein 17.5 
 Solvent 21.2 
R.m.s deviations  
 Bond lengths 0.006Å 
 Bond angles 0.88° 
a

Values in parentheses are for the highest resolution shell (2.35–2.41 Å). One crystal was used for each data set. TLS (translation/libration/screw) parameters, one set for each protomer, were included in the refinement.

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