Table 2.

Crystal structure data collection and refinement statistics

Criteria Cross-linked SHD-Kar3Vik1 
Space group P212121 
Cell dimensions  
a, b, c (Å) 88.1, 94.9, 114.6 
α, β, γ (°) 90, 90, 90 
Wavelength 0.979206 
Resolution (Å)a 25–2.3 (2.34–2.3) 
Rmergea 5.1 (60.1) 
I/σIa 19.7 (3.2) 
Completeness (%)a 99.9 (99.8) 
Redundancya 8.6 (6.2) 
Resolution (Å)a 25–2.3 (2.34–2.3) 
No. reflectionsb 40710 (2701) 
Rwork/Rfreec 0.21/0.24 
No. atoms  
Protein 5361 
Water 246 
Average B-factors2 
Protein 69.991 
Water 54.972 
R.m.s. deviations  
Bond lengths (Å) 0.005 
Bond angles (°) 0.891 
PDB accession no. 4ETP 
Criteria Cross-linked SHD-Kar3Vik1 
Space group P212121 
Cell dimensions  
a, b, c (Å) 88.1, 94.9, 114.6 
α, β, γ (°) 90, 90, 90 
Wavelength 0.979206 
Resolution (Å)a 25–2.3 (2.34–2.3) 
Rmergea 5.1 (60.1) 
I/σIa 19.7 (3.2) 
Completeness (%)a 99.9 (99.8) 
Redundancya 8.6 (6.2) 
Resolution (Å)a 25–2.3 (2.34–2.3) 
No. reflectionsb 40710 (2701) 
Rwork/Rfreec 0.21/0.24 
No. atoms  
Protein 5361 
Water 246 
Average B-factors2 
Protein 69.991 
Water 54.972 
R.m.s. deviations  
Bond lengths (Å) 0.005 
Bond angles (°) 0.891 
PDB accession no. 4ETP 
a

Data in parentheses represent the highest resolution shell.

b

Data in parentheses represent the number of reflections used for the calculation of Rfree.

c

Rfactor = ∑|FobsFcalc| / ∑|Fobs|.

Where Rwork refers to the Rfactor for the data utilized in the refinement and Rfree refers to the Rfactor for 5% of the data that were excluded from the refinement.

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